This Pumpkin Spice soap has clove, vetiver, ginger, anise and patchouli EOs with vanilla oleoresin - a TON of IFRA math involved!
So it's Fall and those spicy essential oils come a-callin' to be made into some yummy, delicious soaps. Tis the season - they deserve to be in your shower!
Not so fast! Despite what many in the essential oil industry may lead you to believe, there *is* a guideline for safe essential oil use on your skin, even in soap. There's a limit that's set forth by the IFRA (International Fragrance Association) - you can find them at www.ifraorg.org. Some suppliers do the work for you and provide their own IFRA certificates for their essential oils. Check with your essential oil supplier for this information first as it will save you a TON of time!
But what if your supplier doesn't supply this information? Well that's when you'll need to figure out your oil's limits on your own with the IFRA.
And that's when stuff gets real. How do you use this BLASTED website? I just want to know how much clove essential oil I can put into my cinnamon clove soap! Geesh! Well, gentle soaper, I am here to help you on your way. Here's the steps I generally go through to determine the UPPER LIMIT for essential oil usage in my soap. This isn't to say that you can't use less - it's just the top of the range is all. I like to both write on the labels on my essential oil bottles and keep a running list in the back of my soap journal of each of the usage rates I've already noodled out. I suggest doing the same so you're not going through this all the time!
First, a word on essential oils and the things to look for when buying them. You'll see why we need a supplier that gives you all of the following information once we dig into the usage rates with the IFRA. We will need to be using essential oil suppliers who readily provide you with the following information:
- Botanical name of the
plant the EO originated from. This is a latin name - for clove bud, we're looking for "Syzygium aromaticum L." This is how we know that we are *all* talking about the same plant here.
- Gas Chromatography/Mass Spectrometry lab report (GC/MS). This report gives you a breakdown of what is in the essential oil - normally a combination of terpenes, aldehydes, esters, phenols, oxides, alcohols and ketones. It should also give you the percentages of these components within the oil - so you know WHAT and HOW MUCH of each constituent is in your essential oil.
These are bare bones. I also like to have country of origin, the part of the plant that the EO was distilled from (leaf, fruit, bark, root, etc), and the method of extraction (steam, CO2, cold pressed). All of these affect the aromatic quality of the oil and, in some cases, the makeup of the oil's profile.
So let's get down to business!
From here on out, I'm going to use
Clove Bud (Indonesia) essential oil from New Directions Aromatics (NDA) as my example. There is a .pdf of the oil's GC/MS report
here.
The document you'll want (NEED!) from the IFRA is
this one. Keep in mind that these standards are always being reviewed and reevaluated. An oil that's OK at one usage rate today may not be next year. I check about every 6 months or so to make sure I'm still in the right range. That might be too often, and generally you'll hear some noise-making about a popular oil's rate being changed. I just happen to be a particular brand of careful (husband might say paranoid) so I check often!
OK, back to clove! According to that GC report, this clove EO has 73.6% straight Eugenol - that's the main component of this oil. There's an additional 4.7% Eugenyl Acetate on the report - for the purposes of the IFRA, you'll find that they're both the "same thing" as far as their restriction goes. So we'll say that for this clove bud essential oil, we're dealing with 78.3% Eugenol. I like to always round UP whenever I see a decimal, because as you saw above, I'm a Nervous Nelly! So we'll call it at
79% Eugenol.
Now go to your IFRA .pdf document. Type ctrl + F. There should be a search box in the upper right. Type "Eugenol" in. You'll come across an entry with a heading that says "Eugenol" - on the .pdf file, it's on page 180.
The thing to look for here is that 1) Yes, it is Restricted and 2) The box of categories with the usage rates restrictions. For the purposes of soapmaking, we want category 9 - which is for bar soap (also liquid soap and other things). In a
finished product, we can only have
0.5% Eugenol total.
OK! So now it's time for some math. Let's say you're about to make a 2 lb loaf of soap. I like to work in grams, and you'll see why in a minute. Two pounds of soap translates to about 905 grams total. This is your FINISHED soap (cured) - so if you're looking at your recipe of oils and additives, then I would add up everything except your liquid to get your total. As we all know, that liquid evaporates out and would therefore make all the other ingredients that much more concentrated - including that eugenol. So just take that out of your equation. We'll pretend that the 905 grams of soap is already minus our liquid. Ready for the math? Here goes:
0.5% of 905 grams (0.005 * 905) is
4.52 grams. That's the
most Eugenol you can have in your soap. See why I used grams? That's a fraction of an ounce right there, so the smaller measurement will be more accurate.
To find out how much total clove bud oil we can use, you'll need to divide by the percentage of Eugenol (79%) we found in our Clove Bud oil. So: 4.52 / 0.79 = 5.721518987341772
ROUND DOWN. Unless you have a special scale that is great at reading those fractions of a gram, of course. I don't have such fancy things, so I round down to be safe. For this soap, you can only use
5 grams of this Clove Bud oil.
Now, if you have a smaller fraction than that and you want an easy way to measure those fractions without a fancy scale, you can always create a dilution. Let's say that getting to that .7 of a gram is really important to you and your blend. Do a 10% dilution of EO into a carrier oil that is in your soaping oils (let's say olive). So you can use 5 grams of your straight clove bud oil and 7 grams of your 10% dilution in olive oil to get pretty darned close!
And that's how you get your UPPER LIMIT from the IFRA for your oils. I used the upper limit in the soap pictured above (actually a little less!) and I can still smell it. Clove is actually quite potent! And now I know that, unless I come across a particularly sensitive/allergic person, my soap is generally safe for use. Whew!
A few more things to mention:
The reason you'll want to know the PART of the plant used for gathering the essential oil is that the oil's profile can vary widely, even on the same botanical name! For example, to compare to the clove bud above, there's also clove LEAF essential oil, which has a higher Eugenol rate (about 86%). You'll find the same goes with cinnamon LEAF v. BARK. For a higher usage, go with clove bud and cinnamon leaf. Bear in mind that the main sensitizer in cinnamon leaf is ALSO Eugenol, so you'll want to watch the total content of Eugenol in your recipe if you use both of these oils.
The other IFRA categories refer to other types of products you may also be making, including (but not limited to) lip products, lotions, shaving, toothpaste, and products for babies/children. Page 12 of
this .pdf has an exhaustive list of these categories and which products they contain. So you can do the same calculations as this for any product - but definitely include the water content in your lotions and such!
Some oils are harder to figure out - a lot of folks ran into trouble with Star Anise and Aniseed essential oils: both are different botanical names - different plants - but similar profiles/aromatic scent due to the Anethole content in both. But look for "Anethole" in the IFRA .pdf and it's not there, despite being on the GC/MS reports from NDA for those oils. This is where having references like Robert Tisserand's book (
Essential Oil Safety) become very useful. In it, you'll find that the sensitizer in these oils is anisyl alcohol - which IS listed in the IFRA's document. Some oils require a bit more digging in order to find them - and this is where a certified aromatherapist and resources that are written by/used by aromatherapists and chemists alike can actually come in handy!
And now, a warning (you knew it was coming!): Some oils are just plain not meant for soaping (or for any other use on your body). Some of them can be rectified to remove the compound that's banned (for example: Cade essential oil is nearly ALWAYS rectified to remove the carcinogen that naturally occurs in this oil). Bitter Almond can come FFPA (Free From Prussic Acid - aka cyanide). Some EOs, unfortunately, are irredeemable. These would include wintergreen (99% methyl salicylate - or SUPER concentrated aspirin; one drop is about 3 adult dose aspirin pills), fig leaf and wormwood, among others. Please do your research on the risks of every essential oil you are interested in. Again, Tisserand's book here is a great resource.
And one final note: I am a soapmaker. I am not an aromatherapist, not a professional in the fragrance industry, and not at all a medical professional. This is info I've managed to cobble together from various forums on the web in addition to a few books. If you find anything that's not accurate, PLEASE let me know. You can either comment or email me at jen.ohtc@gmail.com. I'm happy to admit where I'm wrong and fix it so we're not perpetuating any blind leading the blind around here! While I have a lot of knowledge on essential oils, I also know enough to know I don't know everything and that's OK - it's what makes them so much fun! Always learning something new!
And to think I thought I left behind all math and chemistry years ago. Ha! :-)